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81.
Meijuan Xu Zhina Qiao Genshu Huang Mengfei Long Taowei Yang Xian Zhang Minglong Shao Zhenghong Xu Zhiming Rao 《Journal of separation science》2020,43(14):2936-2948
l ‐Arginine has many special physiological and biochemical functions, with wide applications in the food and pharmaceutical industry. Few studies on the purification of l ‐arginine from fermentation broth have been conducted; however, none of them were systematic enough for industrial scale‐up. Therefore, it is necessary to develop a highly efficient and systematic process for the purification of l ‐arginine from fermentation broth. In this study, we screened out a cation exchange resin, D155, having high exchange capacity, high selectivity, and easy elution capacity, and analyzed its adsorption isotherm, thermodynamics, and kinetics using different models. Further, the process parameters of fixed‐bed ion exchange adsorption and elution were optimized, and the penetration curve during the operation was modeled. Based on the fixed‐bed ion‐exchange parameters, a 30‐column continuous ion‐exchange system was designed, and the flow velocity in each zone was optimized. Finally, to obtain a high purity of l ‐arginine, the purification tests were conducted using anion exchange resin 711, and an l ‐arginine yield of 99.1% and purity of 98.5% was obtained. This effective and economical method also provides a promising strategy for separation of other amino acids from the fermentation broth, which is of great significance to the l ‐arginine fermentation industry. 相似文献
82.
建立了一种利用连续流动-分光光度法测定固废中氰化物的浸出毒性的方法,当氰化物浓度在0~200μg/L范围内,校准曲线的相关系数r为0.9998;方法的检出限可以达到0.33μg/L;不同浓度样品测定的相对标准偏差低于2.6%,实际固体废物样品加标回收率为96%~103%,方法精密度良好并且准确度较高;通过实际样品测定结果比对,证明方法与传统国家标准方法测定结果有着较高的吻合度,具有良好的应用前景。 相似文献
83.
84.
Solar Hydrogen from an Aqueous,Noble‐Metal‐Free Hybrid System in a Continuous‐Flow Sampling Reaction System 下载免费PDF全文
Dr. Xiaobo Li Dr. Antony J. Ward Prof. Anthony F. Masters Prof. Thomas Maschmeyer 《Chemistry (Weinheim an der Bergstrasse, Germany)》2014,20(24):7345-7350
We introduce the visible‐light photocatalytic H2 evolution reaction as catalyzed by a cobaloxime/carbon nitride (C3N4) noble‐metal‐free hybrid photosystem by using a continuous‐flow sampling reaction system. The photocatalytic H2 evolution rate is highly dependent on the structure of C3N4, in which porous C3N4 shows the best activity compared with bulk C3N4 (lamellar) and C3N4 nanosheets. When using porous C3N4, the system is neither affected by the solution pH, nor the C3N4 concentration, nor the structure of the cobaloxime complex. 相似文献
85.
Belmesnaoui Aqzzouz Aziz Elbour 《Journal of Mathematical Analysis and Applications》2009,354(1):295-300
We characterize Banach lattices for which each positive Dunford-Pettis operator is M-weakly compact (resp. L-weakly compact) and we give some consequences. 相似文献
86.
We construct an example of a nonseparable Banach space which does not admit a support set.2 It is a consistent (and necessarily independent from the axioms of ZFC) example of a space C(K) of continuous functions on a compact Hausdorff K with the supremum norm. The construction depends on a construction of a Boolean algebra with some combinatorial properties. The space is also hereditarily Lindelöf in the weak topology but it doesn't have any nonseparable subspace nor any nonseparable quotient which is a C(K) space for K dispersed. 相似文献
87.
The pool adjacent violators (PAV) algorithm is an efficient technique for the class of isotonic regression problems with complete
ordering. The algorithm yields a stepwise isotonic estimate which approximates the function and assigns maximum likelihood
to the data. However, if one has reasons to believe that the data were generated by a continuous function, a smoother estimate
may provide a better approximation to that function.
In this paper, we consider the formulation which assumes that the data were generated by a continuous monotonic function obeying
the Lipschitz condition. We propose a new algorithm, the Lipschitz pool adjacent violators (LPAV) algorithm, which approximates
that function; we prove the convergence of the algorithm and examine its complexity.
The authors were supported by the Intramural Research Program of NIH, National Library of Medicine. 相似文献
88.
Using the framework of ordered categories, the paper considers a generalization of the fuzzification machinery of algebraic structures introduced by Rosenfeld as well as provides a new approach to fuzzification of topological structures, which amounts to fuzzifying the underlying “set” of a structure in a suitably compatible way, leaving the structure itself crisp. The latter machinery allows the so-called “double fuzzification”, i.e., a fuzzification of something that is already fuzzified. 相似文献
89.
常见连续型统计分布的一点注记 总被引:1,自引:0,他引:1
正态分布是概率论与数理统计中最重要的一个分布,本文讨论了常见的连续型统计分布与标准正态分布间的关系,结果表明:几乎所有的常见连续型统计分布都是标准正态分布的函数. 相似文献
90.
We introduce an iterative procedure for finding a point in the zero set (a solution to 0 ∈ A(v) and v ∈ C) of an inverse-monotone or inverse strongly-monotone operator A on a nonempty closed convex subset C in a uniformly smooth and uniformly convex Banach space. We establish weak convergence results under suitable assumptions.
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